Synthesis of High-silica Aluminosilicate Zeolites by Peter A
Synthesis of the zeolites on the lightweight aluminosilicate ..
Synthesis of High-Silica Aluminosilicate Zeolites …
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Synthesis of High-Silica Aluminosilicate Zeolites
AB - Seed-assisted methods have provided a new route for the organic structure-directing agent (OSDA)-free synthesis of industrially valuable zeolites. In the present study, we have reported the discovery of the OSDA-free synthesis of ZSM-12 (MTW-type zeolite) by adding calcined zeolite beta seed crystals to the OSDA-free Na-aluminosilicate gel. Various parameters in this synthesis have been comprehensively investigated. Characterization by XRD, FE-SEM, ICP-AES, and 27Al MAS NMR showed that the obtained MTW products without impurity (SiO 2/Al 2O 3 = 31.8-46.4) possessed high crystallinity and a well-defined rod-like morphology. Adsorption-desorption isotherm of water and NH 3-TPD profiles of MTW product showed enough adsorption capacity for water and ammonia molecules, respectively. Moreover, considering the crystallization behavior of seeded and non-seeded Na-aluminosilicate gels, the following key factors were found for inducing the crystallization of MTW by zeolite beta seeds under the hydrothermal condition: the structural similarity between seeds and target zeolite, and the initial gel compositions that provide specific aluminosilicate precursors for the crystallization of MTW prior to the spontaneous nucleation of other zeolite. This methodology provides a promising approach toward designed syntheses of valuable zeolites under environmentally benign conditions.
N2 - Seed-assisted methods have provided a new route for the organic structure-directing agent (OSDA)-free synthesis of industrially valuable zeolites. In the present study, we have reported the discovery of the OSDA-free synthesis of ZSM-12 (MTW-type zeolite) by adding calcined zeolite beta seed crystals to the OSDA-free Na-aluminosilicate gel. Various parameters in this synthesis have been comprehensively investigated. Characterization by XRD, FE-SEM, ICP-AES, and 27Al MAS NMR showed that the obtained MTW products without impurity (SiO 2/Al 2O 3 = 31.8-46.4) possessed high crystallinity and a well-defined rod-like morphology. Adsorption-desorption isotherm of water and NH 3-TPD profiles of MTW product showed enough adsorption capacity for water and ammonia molecules, respectively. Moreover, considering the crystallization behavior of seeded and non-seeded Na-aluminosilicate gels, the following key factors were found for inducing the crystallization of MTW by zeolite beta seeds under the hydrothermal condition: the structural similarity between seeds and target zeolite, and the initial gel compositions that provide specific aluminosilicate precursors for the crystallization of MTW prior to the spontaneous nucleation of other zeolite. This methodology provides a promising approach toward designed syntheses of valuable zeolites under environmentally benign conditions.
Synthesis of High-Silica Aluminosilicate Zeolites - …
Zeolite-like materials have structures similar to zeolites but elements other than Si, Al and O can be present in them. For example, the isoelectronic substitution of 2Si → Al + P has led to the discovery of a wide range of AlPO structures and related phosphate materials . Considerable success have been done recently on making tetrahedral frameworks with the congeners of Al and Si in the next row of the periodic table, namely, Ga and Ge , and only recently the first chiral germanosilicate ITQ-37 has the been discovered with a zeolite-like framework consisting entirely of tetrahedrally coordinated positions occupied by germanium and silicon . Although hundreds of laboratories are trying to synthesize new materials with novel zeolite framework structures, only 191 zeolite framework types have been approved by the .
Molecular sieves are synthetically made zeolites (naturally occurring aluminosilicate minerals), which are having definite pores and uniform dimensions cavities. It has three dimensional structures of silicon dioxide (Sio2) and aluminium oxide (AlO4), which is internally connected. Molecular sieve 13x is the sodium form of the type X crystal and is having pore diameter of 10A° (1.0nm). It will adsorb molecules with a kinetic pore diameter of less than 10 Angstrom and excludes those larger.
Download Synthesis Of High Silica Aluminosilicate Zeolites 1987
Clare Grey - Stony Brook University
ChemInform Abstract: Synthesis of Aluminosilicate Zeolites and Related Silica-Based Materials
PDF Downloads : Oriental Journal of Chemistry
ASDN - Chemistry - Zeolites
Molecular Sieve 13X | Mercaptan Gas Removal
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